In Preparation

When noble metals aren’t so noble:  ambient oxidation of ultrasmall nanoparticles

Lipp, J., Banerjee, R., Patwary, MD. F., Patra, N., Dong, A., Bare, S., Girgsdies, F., and Regalbuto, J. R. “When noble metals aren’t so noble:  ambient oxidation of ultrasmall nanoparticles” in preparation.

Supported Metal-Acid Bifunctional Catalysts Synthesized by Electrostatic Adsorption of Pd onto Metal-Doped Silicas

Anhua Dong, Jake Tillou, John Meynard Tengco, Ananad Ramanthan, John R. Regalbuto. Supported Metal-Acid Bifunctional Catalysts Synthesized by Electrostatic Adsorption of Pd onto Metal-Doped Silicas. In Preparation

Synthesis of Ultra-Small PdAu Nanoparticles with Homogenous Alloys on SiO2 and Al2O3 via Electrostatic Adsorption

Anhua Dong, Douglas A. Blom, John R. Regalbuto. Synthesis of Ultra-Small PdAu Nanoparticles with Homogenous Alloys on SiO2 and Al2O3 via Electrostatic Adsorption. In Preparation.

The Simple Synthesis of High Metal Loading Single Atom Catalysts Via Chelate Fixation

N. Shakouri, H. Adabi, W. Mustain, S. Karakalos, C. Williams, J.R. Regalbuto, “The Simple Synthesis of High Metal Loading Single Atom Catalysts Via Chelate Fixation”, in preparation

The Roles of Metal Loading and Final pH on Silica Supported Pt Particle Size

K. McNamera, A. Shakouri, and J.R. Regalbuto, “The Roles of Metal Loading and Final pH on Silica Supported Pt Particle Size” In preparation.

Comparison of Hydrogenation Activity Pd Particles Supported on Carbon and Oxides

Shakya, R. Banerjee, S. Farzandh, N. Acharya, J. R. Regalbuto and D. A. Chen, “Comparison of Hydrogenation Activity Pd Particles Supported on Carbon and Oxides.” In preparation.

Accurate Subtraction and Deconvolution of Pt Nanoparticles from Crystalline Supports Using Powder XRD with a High Sensitivity Detector

Liu, Q., Tengco, J.M.M., Banerjee, R., Keels, J., and Regalbuto, J.R., Accurate Subtraction and Deconvolution of Pt Nanoparticles from Crystalline Supports Using Powder XRD with a High Sensitivity Detector, in preparation.

Promotion of Silica Supported Cobalt Fischer-Tropsch Catalysts with Minute Amounts of Pt

Almalki, F., Cao, C., Monnier, J.R., and Regalbuto, J.R., Promotion of Silica Supported Cobalt Fischer-Tropsch Catalysts with Minute Amounts of Pt (2021).

2024

The Efect of Reduction Pretreatments on the Size of Supported Pt and Pd Nanoparticles Prepared by Strong Electrostatic Adsorption

Md. Fakhruddin Patwary · Manuel Neito  · Alaba Ojo  · John R. Regalbuto, Catalysis Letters, 24 February 2024

Online Article |

2023

Heterogenization of a Tungstosilicic Acid Catalyst for Esterification of Bio-Oil Model Compound

Prasertpong, P.; Lipp, J.; Dong, A.; Tippayawong, N.; Regalbuto, J.R. Heterogenization of a Tungstosilicic Acid Catalyst for Esterification of Bio-Oil Model Compound. Catalysts 202313, 38.

Online Article |

The preparation of silica supported, dilute limit PdAu alloys via simultaneous strong electrostatic adsorption

Dong, Anhua; Shakouri, Abolfazl; Karakalos, Starvros; Blom, Doug; Williams, CT; REgalbuto, JR

Online Article |

2022

Stabilization of Ultrasmall Platinum Nanoparticles by Nitrogen-Doped Carbon: Implications for Catalysis and Electrocatalysis

Fahim B. A. Rahman, Huynh N. Tien, H. Colon-Mercado, Prabhu Ganesan, Mark C. Elvington, Jay B. Gaillard, Stavros G. Karakalos, and John R. Regalbuto
ACS Applied Nano Materials 2022 5 (8), 10292-10302
Online Article |
Extension of Rietveld Refinement for Benchtop Powder XRD Analysis of Ultrasmall Supported Nanoparticles

Jeremiah Lipp; Ritubarna Banerjee; Md. Fakhruddin Patwary; Nirmalendu Patra; Anhua Dong; Frank Girgsdies; Simon R. Bare and J. R. Regalbuto “Extension of Rietveld Refinement for Benchtop Powder XRD Analysis of Ultrasmall Supported NanoparticlesChem. Mater. 2022, 34, 18, 8091–8111

Online Article |

Dilute Limit Alloy Pd-Cu Bimetallic Catalysts Prepared by Simultaneous Strong Electrostatic Adsorption: A Combined Infrared Spectroscopic and Density Functional Theory Investigation

L.T. De Castro, D. Sahsah, A. Heyden, C.T. Williams and J.R. Regalbuto. Dilute Limit Alloy Pd-Cu Bimetallic Catalysts Prepared by Simultaneous Strong Electrostatic Adsorption: A Combined Infrared Spectroscopic and Density Functional Theory Investigation. J. Phys. Chem. C (Accepted for publication, 2022).

All the lonely atoms, where do they all belong?

Regalbuto, J.R., Datye, A.K. All the lonely atoms, where do they all belong?. Nat. Nanotechnol. (2022)

The extension of Rietveld refinement for benchtop powder XRD analysis of ultra-small supported nanoparticles

Lipp, J., Patwary, M.D. F., Patra, N., Dong, A., Girgsdies, F., Bare, S., and Regalbuto, J. R. “The extension of Rietveld refinement for benchtop powder XRD analysis of ultra-small supported nanoparticles” under review for Chemistry of Materials (2022).

2021

Supported nanoparticle synthesis with Au bis-Ethylenediamine: The mechanism of adsorption onto oxides and carbons

Sean R. Noble, Sean E. Barnes, Ritubarna Banerjee, Jeff Miller, John R. Regalbuto, Supported nanoparticle synthesis with Au bis-Ethylenediamine: The mechanism of adsorption onto oxides and carbons, Journal of Catalysis, Volume 393, 2021, Pages 344-356

The stabilization of supported Au nanoparticles in a highly sintering environment using high surface free energy Pt and Ru cores

Kerry C O’Connell, John R Monnier, JR Regalbuto, The stabilization of supported Au nanoparticles in a highly sintering environment using high surface free energy Pt and Ru cores, JOURNAL OF MATERIALS CHEMISTRY A, Volume 9, Issue 40, Page 23223-23233 (2021)

Mixing optimization with inward flow configuration contra-rotating impeller, baffle-free tank

“P. Satjaritanun, J.R. Regalbuto, J.A. Regalbuto, N. Tippayawong, S. Shimpalee, Mixing optimization with inward flow configuration contra-rotating impeller, baffle-free tank, Alexandria Engineering Journal, Volume 60, Issue 4, 2021, Pages 3759-3779”

High-performing commercial Fe–N–C cathode electrocatalyst for anion-exchange membrane fuel cells

Adabi, H., Shakouri, A., Ul Hassan, N. et al. High-performing commercial Fe–N–C cathode electrocatalyst for anion-exchange membrane fuel cells. Nat Energy 6, 834–843 (2021).

Understanding how single-atom site density drives the performance and durability of PGM-free Fe-N-C cathodes in anion exchange membrane fuel cells

Horie Adabi, Pietro Giovanni Santori, Abolfazl Shakouri, Xiong Peng, Karam Yassin, Igal G. Rasin, Simon Brandon, Dario R. Dekel, Noor Ul Hassan, Moulay-Tahar Sougrati, Andrea Zitolo, John R. Varcoe, John R. Regalbuto, Frédéric Jaouen, William E. Mustain, Understanding how single-atom site density drives the performance and durability of PGM-free Fe–N–C cathodes in anion exchange membrane fuel cells, Materials Today Advances, Volume 12, 2021

Cs-RHO Goes from Worst to Best as Water Enhances Equilibrium CO2 Adsorption via Phase Change

Xu, L., Okrut, A., Tate, G. L., Ohnishi, R., Wu, K.-L., Xie, D., Kulkarni, A. R., Takewaki, T., Monnier, J. R., Katz, A. (2021). Cs-RHO Goes from Worst to Best as Water Enhances Equilibrium CO2 Adsorption via Phase Change. Langmuir

Supported nanoparticle synthesis with Au bis-Ethylenediamine: The mechanism of adsorption onto oxides and carbons

Noble, S.R., Barnes, S.A., Banerjee, R., Miller, J. and Regalbuto, J.R., Supported Nanoparticle Synthesis with Au bis-Ethylenediamine: The Mechanism of Adsorption Onto Oxides and Carbons, Journal of Catal., 2021, 393, 344–356. https://doi.org/10.1016/j.jcat.2020.11.026

2020

Rectifying the Chemisorption – XRD Discrepancy of Carbon Supported Pd:  Residual Chloride and/or Carbon Decoration

Banerjee, R., and Regalbuto, J.R., Rectifying the Chemisorption – XRD Discrepancy of Carbon Supported Pd:  Residual Chloride and/or Carbon Decoration, Appl. Catal. A-General, 2020, 595, 117504. https://doi.org/10.1016/j.apcata.2020.117504

Rational Synthesis of Bimetallic Catalysts Using Electroless Deposition Methods

Diao, W., Tengco, J.M.M.T., Gaffney, A.M., Regalbuto, J.R., and Monnier, J.R., Rational Synthesis of Bimetallic Catalysts Using Electroless Deposition Methods, in Catalysis 2020, 32, Volume 32, Spivey, J.J. ed., in press. https://doi.org/10.1039/9781788019477-00116

Optimization of Process Variables for Esterification of Bio-Oil Model Compounds by a Heteropolyacid Catalyst

Prasertpong, P., Jaroenkhasemmeesuk, C., Regalbuto, J.R., Lipp, J.,  and Tippayawong, N., Optimization of Process Variables for Esterification of Bio-Oil Model Compounds by a Heteropolyacid Catalyst, Ener. Rep. 2020, 6, 1. https://doi.org/10.1016/j.egyr.2019.11.026

An Analysis of Electroless Deposition Derived Ni-Pt Catalysts for the Dry Reforming of Methane

Egelske, B.T., Keels, J.M., Monnier, J.R., and Regalbuto, J.R., An Analysis of Electroless Deposition Derived Ni-Pt Catalysts for the Dry Reforming of Methane, J. Catal. 2020, 381, 374-384. https://doi.org/10.1016/j.jcat.2019.10.035

2019

Preparation of Pt/Graphene Catalysts for Polymer Electrolyte Membrane Fuel Cells by Strong Electrostatic Adsorption Technique

Pothaya, S., Regalbuto, J.R., Monnier, J.R., and Punyawudho, K., Preparation of Pt/Graphene Catalysts for Polymer Electrolyte Membrane Fuel Cells by Strong Electrostatic Adsorption Technique, Intl. J. Hyd. Ener.  2019, 44, 26361. https://doi.org/10.1016/j.ijhydene.2019.08.110

Pushing the limits electrostatic adsorption: charge enhanced dry impregnation of SBA-15

Eskandari, S., Dong, A.H., De Castro, L.T., Rahman, F.B.B., Lipp, J., Blom, D., and Regalbuto, J.R., Pushing the limits electrostatic adsorption: charge enhanced dry impregnation of SBA-15, Catal. Tod., 2019, 338, 60. https://doi.org/10.1016/j.cattod.2019.06.082

Aqueous phase hydrogenation of succinic acid using bimetallic Ir-Re/C catalysts prepared by strong electrostatic adsorption

Keels, J.M., Chen, X., Karakalos, S., Liang, C.H., Monnider, J.R., and Regalbuto, J.R., Aqueous phase hydrogenation of succinic acid using bimetallic Ir-Re/C catalysts prepared by strong electrostatic adsorption, ACS Catal. 2019, 8, 6486. https://doi.org/10.1021/acscatal.8b01006

The Use of Salts to Control Silica Supported Pt Particle SAize in Charge Enhanced Dry Impregnation

Eskandari, S., Li, Y.T., Tao, F.F., and Regalbuto, J.R., The Use of Salts to Control Silica Supported Pt Particle SAize in Charge Enhanced Dry Impregnation, Catal. Tod., 2019, 334, 187. https://doi.org/10.1016/j.cattod.2018.11.033

2018

Nanoparticle synthesis via electrostatic adsorption using incipient wetness impregnation

Eskandari, S., Tate, G., Leaphart, N., and Regalbuto, J.R., Nanoparticle synthesis via electrostatic adsorption using incipient wetness impregnation, ACS Catal. 2018, 8, 10, 383. https://doi.org/10.1021/acscatal.8b03435

Ambient Oxidation of Ultrasmall platinum nanoparticles on microporous carbon catalyst supports

Banerjee, R., Chen, D.A., Karakalos, S. Piedboeu, M.L.C., Job, N., and Regalbuto, J.R., Ambient Oxidation of Ultrasmall platinum nanoparticles on microporous carbon catalyst supports, ACS Appl. Nanomat., 2018 1, 5876. https://doi.org/10.1021/acsanm.8b01548

Electrostatic Adsorption of Platinum onto Carbon Nanotubes and Nanofibers for Nanoparticle Synthesis

Banerjee, R., Contreras-Mora, J. L., McQuiston, S. K., Bolton, B., Mehrabi B.A.T., and J. R. Regalbuto, “Electrostatic Adsorption of Platinum onto Carbon Nanotubes and Nanofibers for Nanoparticle Synthesis,” J. Carbon Res. 2018, 4, 12. https://doi.org/10.3390/c4010012

A Simple Synthesis of Highly Dispersed, Homogeneously Alloyed, Supported Bimetallic Nanoparticles

Wong, A., Liu, Q., Griffin, S., Nichols, A., and Regalbuto, J.R., A Simple Synthesis of Highly Dispersed, Homogeneously Alloyed, Supported Bimetallic Nanoparticles, Science, 2018, 358, 1427

Experimental and Computational Investigation of Mixing with Contra-Rotating, Baffle-Free Impellers

Satjaritanum, P., Bringley, E., Weidner, J.W., Khunatorn, Y., Regalbuto, J.A., Regalbuto, J.R., and Shimpalee, S., Experimental and Computational Investigation of Mixing with Contra-Rotating, Baffle-Free Impellers, Chem. Eng. Res. Des. 2018, 130, 63. https://doi.org/10.1016/j.cherd.2017.12.010

The Sintering and Active Sites of Supported Gold Catalysts for the Hydrodechlorination of Acetylene

O’Connell, K. C., Monnier, J.R., and Regalbuto, J.R., The Sintering and Active Sites of Supported Gold Catalysts for the Hydrodechlorination of Acetylene, Appl. Catal. B. Env., 2018, 225, 264

The curious relationship of sintering to activity in supported gold catalysts for the hydrochlorination of acetylene

O’Connell, K. C., Monnier, J.R., and Regalbuto, J.R., The curious relationship of sintering to activity in supported gold catalysts for the hydrochlorination of acetylene, Appl. Catal. B. Env., 2018, 225, 264

Electrostatic adsorption-microwave synthesis of palladium nanoparticles on graphene for improved cross-coupling activity

Gilliland, S.E., Tengco, J.M.T., Yang, Y., Regalbuto, J.R., Castano, C.E., and Gupton, B.F., Electrostatic adsorption-microwave synthesis of palladium nanoparticles on graphene for improved cross-coupling activity, Applied Catalysis A: General 2018, 550, 168. https://doi.org/10.1016/j.apcata.2017.11.007

A Review of Preparation Methods for Supported Metal Catalysts, Advances in Catalysis

Tavakoli, B., Eskandari, S., Khan, U., White, R.D., and Regalbuto, J.R., A Review of Preparation Methods for Supported Metal Catalysts, Adv. Catal., 2017, 61, 1. https://doi.org/10.1016/bs.acat.2017.10.001

Electrostatic Adsorption for the Synthesis of Highly Active Bimetallic Au/Pd/Carbon Catalysts for Benzyl Alcohol Oxidation

Cho, H.R., Barnes, S., Tengco, J.M.M., Shaw, G., Hutchings, G.J., Sanchez, S.I., Bradley, S.A., and Regalbuto, J.R., Electrostatic Adsorption for the Synthesis of Highly Active Bimetallic Au/Pd/Carbon Catalysts for Benzyl Alcohol Oxidation, in preparation.

Understanding Uptake of Pt Precursors During Strong Electrostatic Adosrption on Single-Crystal Carbon Surfaces

Seuser, G.S., Banerjee, R., Metavarayuth, K., Brandt, A.J., Maddamumapatabandi, T.D., Karakalos, S., Lin, Y., Regalbuto, J.R., and Chen, D.A., Understanding Uptake of Pt Precursors During Strong Electrostatic Adosrption on Single-Crystal Carbon Surfaces, Topics in Catalysis 2018, 61, 379. DOI: 10.1007/s11244-017-0872-3

2017

A Simple Synthesis of Highly Dispersed, Homogeneously Alloyed, Supported Bimetallic Nanoparticles

Wong, A., Liu, Q., Griffin, S., Nicholls, A., and Regalbuto, J.R, A Simple Synthesis of Highly Dispersed, Homogeneously Alloyed, Supported Bimetallic Nanoparticles, Science 2017, 358, 6369.

Bio-Oil Hydrodeoxygenation Catalysts Produced Using Strong Electrostatic Adsorption

Elkasabi, Y., Liu, Q., Choi, G. Strahan, Y., Boateng, A.A., and Regalbuto, J.R., Bio-Oil Hydrodeoxygenation Catalysts Produced Using Strong Electrostatic Adsorption, Fuel 2017, 207, 510. https://doi.org/10.1016/j.fuel.2017.06.115

Using Polyfurfural Alcohol to Improve the Hydrothermal Stability of Mesoporous Oxides for Reactions in the Aqueous Phase

Chung, S., Liu, Q., Joshi, U., Regalbuto, J.R., Boateng, A.A., Coe, C., and Smith, M., Using Polyfurfural Alcohol to Improve the Hydrothermal Stability of Mesoporous Oxides for Reactions in the Aqueous Phase, J. Porous Mater. 2017, 25, 407. DOI: 10.1007/s10934-017-0451-9

Detection of Ambient Oxidation of Ultrasmall Supported Pt Nanoparticles with Benchtop Powder X-ray Diffraction

Banerjee, R., Liu, Q., Tengco, J.M.M., and Regalbuto, J.R., Detection of Ambient Oxidation of Ultrasmall Supported Pt Nanoparticles with Benchtop Powder X-ray Diffraction, Catal. Lett., 2017 147, 1754. DOI: 10.1007/s10562-017-2060-2

Continuous Flow Synthesis of Cu@M (M=Ni, Co) Core/Shell Nanocomposites

Smith, S.E., Zachary, J., Huba, Z.H., Fahad Almalki, F., Regalbuto, J.R., Monnier, J.R., and Carpenter, E.C., Continuous Flow Synthesis of Cu@M (M=Ni, Co) Core/Shell Nanocomposites, J. Flow Chem., 2017, 7, 18. https://doi.org/10.1556/1846.2016.00037

A Pinch of Salt to Control Supported Pt Nanoparticle Size

Liu, Q., Samad, J., Copple, J.E., Eskandari, S., Satterwhite, C., and Regalbuto, J.R., A Pinch of Salt to Control Supported Pt Nanoparticle Size, Catal. Tod. 2017, 280, 246. https://doi.org/10.1016/j.cattod.2016.04.031

2016

Synthesis of Ag Nanoparticles on Oxide and Carbon Supports from Ag Diammine Precursor

Kyriakidou, E.A., Alexeev, O.S., Wong, A.P., Papadimitriou, C., Amiridis, M.D., and Regalbuto, J.R., Synthesis of Ag Nanoparticles on Oxide and Carbon Supports from Ag Diammine Precursor, J. Catal. 2016, 344, 749. https://doi.org/10.1016/j.jcat.2016.08.018

The Controlled Synthesis of Metal-Acid Bifunctional Catalysts: The Effect of Metal:Acid Ratio and Metal-Acid Proximity in Pt Silica-Alumina Catalysts for n-Heptane Isomerization

Samad, J.E., Blanchard, J., Sayag, C., Louis, C., and Regalbuto, J.R., The Controlled Synthesis of Metal-Acid Bifunctional Catalysts: The Effect of Metal:Acid Ratio and Metal-Acid Proximity in Pt Silica-Alumina Catalysts for n-Heptane Isomerization, J.Catal. 2016, 342, 203. https://doi.org/10.1016/j.jcat.2016.08.004

The Controlled Synthesis of Metal-Acid Bifunctional Catalysts: Selective Pt Deposition and Nanoparticle Synthesis on Amorphous Aluminosilicates

Samad, J.E., Blanchard, J., Sayag, C., Louis, C., and Regalbuto, J.R., The Controlled Synthesis of Metal-Acid Bifunctional Catalysts: Selective Pt Deposition and Nanoparticle Synthesis on Amorphous Aluminosilicates, J.Catal. 2016, 342, 213.

Characterization and Evaluation of Pt-Pd Electrocatalysts Prepared by Electroless Deposition

Wongkaew, A., Zhang, Y.Y., Tengco, J.M.M., Blom, D.A., Sivasubramanian, P., Fanson, P.T., Regalbuto, J.R., and Monnier, J.R., Characterization and Evaluation of Pt-Pd Electrocatalysts Prepared by Electroless Deposition, Appl. Catal. B. Env. 2016, 188, 367. https://doi.org/10.1016/j.apcatb.2016.02.022

Synthesis and Electrochemical Evaluation of Carbon Supported Pt-Co Bimetallic Catalysts Prepared by Electroless Deposition and Modified Charge Enhanced Dry Impregnation

Tengco, J.M.M., Mehrabadik, B.A.T., Zhang, Y., Wongkaew, A., Regalbuto, J.R., Weidner, J.W., and Monnier, J.R., Synthesis and Electrochemical Evaluation of Carbon Supported Pt-Co Bimetallic Catalysts Prepared by Electroless Deposition and Modified Charge Enhanced Dry Impregnation, Catalysts 2016, 6, 83. DOI: 10.3390/catal6060083

The Simple, Effective Synthesis of Highly Dispersed Pd/C and CoPd/C Heterogeneous Catalyst via Charge-Enhanced Dry Impregnation

D’Souza, L., Barnes, S., and Regalbuto, J.R., The Simple, Effective Synthesis of Highly Dispersed Pd/C and CoPd/C Heterogeneous Catalyst via Charge-Enhanced Dry Impregnation, Catalysts 2016, 6, 72. https://doi.org/10.3390/catal6050072

The Catalytic Behavior of Precisely Synthesized Pt-Pd Bimetallic Catalysts for Use as Diesel Oxidation Catalysts

Wong, A., Kyriakidou, E., Toops, T., and Regalbuto, J.R., The Catalytic Behavior of Precisely Synthesized Pt-Pd Bimetallic Catalysts for Use as Diesel Oxidation Catalysts, Catal. Tod., 2016, 267, 145. https://doi.org/10.1016/j.cattod.2016.02.011

A Comparison of Pt (II) and Pt (IV) Chloride Precursors for Strong Electrostatic Adsorption Synthesis of Pt/Alumina and Pt/Carbon Catalysts

Samad, J. E., Keels, J., and Regalbuto, J. R., A Comparison of Pt (II) and Pt (IV) Chloride Precursors for Strong Electrostatic Adsorption Synthesis of Pt/Alumina and Pt/Carbon Catalysts. Catal. Lett., 145, 2016, 157. https://doi.org/10.1007/s10562-015-1631-3

2015

Synthesis of Platinum Catalysts over Thick Slurries of Oxide Supports by Strong Electrostatic Adsorption

Samad, J., Hoenig, S., and Regalbuto, J.R., Synthesis of Platinum Catalysts over Thick Slurries of Oxide Supports by Strong Electrostatic Adsorption, ChemCatChem 7, 2015, 5123. https://doi.org/10.1002/cctc.201500595

Preparation and characterization of Pt-Ru Bimetallic Catalysts Synthesized by Electroless Deposition Methods

Diao, W.J., Tengco, J.M.M., Regalbuto, J.R., and Monnier, J.R., Preparation and characterization of Pt-Ru Bimetallic Catalysts Synthesized by Electroless Deposition Methods, ACS Catal. 5, 2015, 5123. https://doi.org/10.1021/acscatal.5b01011

Rational nanoparticle synthesis to determine the effects of size, support, and K dopant on Ru activity for levulinic acid hydrogenation to gamma-valerolactone

Cao, S., Monnier, J.R., Williams, C.T., Diao, W.J., and Regalbuto, J.R., Rational nanoparticle synthesis to determine the effects of size, support, and K dopant on Ru activity for levulinic acid hydrogenation to gamma-valerolactone, J. Catal. 326, 2015, 69. https://doi.org/10.1016/j.jcat.2015.03.004

The Rational Synthesis of Pt-Pd Bimetallic Catalysts by Electrostatic Adsorption

Cho, H.-R. and Regalbuto, J.R., The Rational Synthesis of Pt-Pd Bimetallic Catalysts by Electrostatic Adsorption, Cat. Tod. 246, 2015, 143. https://doi.org/10.1016/j.cattod.2014.09.029

Chemisorption-XRD Particle Size Discrepancy of Carbon Supported Palladium: Carbon Decoration of Pd?

Tengco, J.M.M., Lugo-Jose, Y.K., Monnier, J.R., and Regalbuto, J.R., Chemisorption-XRD Particle Size Discrepancy of Carbon Supported Palladium: Carbon Decoration of Pd?, Cat. Tod. 246, 2015, 9. https://doi.org/10.1016/j.cattod.2014.07.006

High Sensitivity Silicon Slit Detectors for 1 nm Powder XRD Size Detection Limit

O’Connell, K., and Regalbuto, J.R., High Sensitivity Silicon Slit Detectors for 1 nm Powder XRD Size Detection Limit, Catal. Lett. 145, 2015, 777. https://doi.org/10.1007/s10562-015-1479-6

2014

Determining surface composition of mixed oxides with pH

Samad, J., Hashim, S., Ma, S., and Regalbuto, J.R., Determining surface composition of mixed oxides with pH, J. Coll. Interf. Sci. 436, 2014, 204.

In-situ monitoring of transition metal complex adsorption on oxide surfaces during the first stages of supported metal catalyst preparation

Blanchard, J. Hervier, A., Costentin, G., Regalbuto, J., Louis, C., and Boujday, S., In-situ monitoring of transition metal complex adsorption on oxide surfaces during the first stages of supported metal catalyst preparation, Catal. Tod. 235, 2014, 245.

The Control of Pt and Ru Nanoparticle Size on High Surface Area Supports

Liu, Q., Joshi, U., Uber, K., and Regalbuto, J.R., The Control of Pt and Ru Nanoparticle Size on High Surface Area Supports, Phys. Chem. Chem. Phys. 16, 2014, 26431.

The Genesis of a Heterogeneous Catalyst: In Situ Observation of a Transition Metal Complex Adsorbing onto an Oxide Surface in Solution

Hervier, A., Blanchard, J., Costentin, G., Regalbuto, J., Louis, C., and Boujday, S., The Genesis of a Heterogeneous Catalyst: In Situ Observation of a Transition Metal Complex Adsorbing onto an Oxide Surface in Solution, Chem. Comm. 50, 2014, 2409.

2013

Selective Adsorption of Manganese onto Rhodium for Optimized Mn/Rh/SiO2 Alcohol Synthesis Catalysts

Liu, J.J., Tao, R.Z., Guo, Z., Regalbuto, J.R., Marshall, C.L., Klie, R.F., Miller, J.T., and Meyer, R.J., Selective Adsorption of Manganese onto Rhodium for Optimized Mn/Rh/SiO2 Alcohol Synthesis Catalysts, ChemCatChem 5, 2013, 3665.

Charge Enhanced Dry Impregnation: A Simple Way to Improve Preparation of Supported Metal Catalysts

Zhu, X., Cho, H.-R., and Regalbuto, J.R., Charge Enhanced Dry Impregnation: A Simple Way to Improve Preparation of Supported Metal Catalysts, ACS Catalysis 3, 2013, 625.

2012

Molecular Characterization of Noble Metal Adsorption at the Water-Aluminum Oxide Interface

Liu, J., and Regalbuto, J.R., Molecular Characterization of Noble Metal Adsorption at the Water-Aluminum Oxide Interface, Adv. Chem. Eng. 396-398, 2012, 745.

2011

The Sea Change in U.S. Biofuels Funding

Regalbuto, J.R., (Invited Perspective), The Sea Change in U.S. Biofuels Funding, Biofpr 5, 2011, 495.

In-Situ Electron Energy Loss Spectroscopy Study of Mn-Promoted Co/TiO2 Fischer-Tropsch Catalysts

Zhao, Y., Feltes, T.E., Regalbuto, J.R., Meyer, R.J., and Klie, R.F., In-Situ Electron Energy Loss Spectroscopy Study of Mn-Promoted Co/TiO2 Fischer-Tropsch Catalysts, Catalysis Letters 141, 2011, 641.

A Fundamental Study of Pt Impregnation of Carbon: Adsorption Equilibrium and Particle Synthesis

Hao, X., Barnes, S., and Regalbuto, J. R., A Fundamental Study of Pt Impregnation of Carbon: Adsorption Equilibrium and Particle Synthesis, J. Catalysis 279, 2011, 48.

2010

In Situ Electron Energy Loss Spectroscopy Study of Metallic Co and Co Oxides

Zhao Y., Feltes T.E., Regalbuto J.R., Meyer R.J., and Klie R.F., In Situ Electron Energy Loss Spectroscopy Study of Metallic Co and Co Oxides , J. Appl. Phys., 108, 2010, 063704.

The Influence of Preparation Method on Mn-Co Interactions in Mn/Co/TiO2 Fischer-Tropsch Catalysts

Feltes, T. E., Y. Zhao, R.J. Meyer, R. Klie, and Regalbuto, J.R., The Influence of Preparation Method on Mn-Co Interactions in Mn/Co/TiO2 Fischer-Tropsch Catalysts, ChemCatChem 2, 2010, 1065.

An NSF Perspective on Next Generation Hydrocarbon Biorefineries

Regalbuto, J.R., An NSF Perspective on Next Generation Hydrocarbon Biorefineries, Computers & Chem. Eng., 34 , 2010, 1393.

Synthesis and Characterization of Highly Loaded Pt/carbon Xerogel Catalysts Prepared by the Strong Electrostatic Adsorption Method

N. Job, F. Maillard, M. Chatenet, C. J. Gommes,. S. Lambert, S. Hermans, J. R. Regalbuto, and J.-P. Pirard, Synthesis and Characterization of Highly Loaded Pt/carbon Xerogel Catalysts Prepared by the Strong Electrostatic Adsorption Method, Studies in Surface Science and Catalysis 167, 2010, 169.

Strong Electrostatic Adsorption for the Preparation of Pt/Co/C and Pd/Co/C bimetallic Electrocatalysts

D’Souza, L., and Regalbuto, J.R., Strong Electrostatic Adsorption for the Preparation of Pt/Co/C and Pd/Co/C bimetallic Electrocatalysts, Studies in Surface Science and Catalysis 175, 2010, 715.

The Determination of Surface Charging Parameters for a Predictive Metal Adsorption Model

Schreier, M., Timmons, M., Feltes, T., and Regalbuto, J.R., The Determination of Surface Charging Parameters for a Predictive Metal Adsorption Model, Journal of Colloid and Interface Science 348, 2010, 571.

Selective Adsorption of Manganese onto Cobalt for Optimized Mn/Co/TiO2 Fischer-Tropsch Catalysts

T. E Feltes, L. Espinosa-Alonso, E. de Smit, L. D’Souza, R. J. Meyer, B. M Weckhuysen, J. R. Regalbuto , Selective Adsorption of Manganese onto Cobalt for Optimized Mn/Co/TiO2 Fischer-Tropsch Catalysts, J. Catalysis 270, 2010, 95.

Preparation of Highly Loaded Pt/Carbon Xerogel Catalysts for Proton Exchange Membrane Fuel Cells by the Strong Electrostatic Adsorption Method

N. Job, S. Lambert, M. Chatenet, C. J. Gommes, F. Maillard, . Berthon-Fabry, J. R. Regalbuto, J.-P. Pirard, Preparation of Highly Loaded Pt/Carbon Xerogel Catalysts for Proton Exchange Membrane Fuel Cells by the Strong Electrostatic Adsorption Method, Catalysis Today 150, 2010, 119.

2009

Cellulosic Biofuels: Got Gasoline?

Regalbuto, J.R., (Invited Perspective), Cellulosic Biofuels: Got Gasoline?, Science 325, 2009, 822.

Synthesis of Very Highly Dispersed Platinum Catalysts Supported on Carbon Xerogels by the Strong Electrostatic Adsorption Method

S. Lambert, N. Job, L. D’Souza, M. F. R. Pereira, R. Picard, B. Heinrichs, J.L. Figuerido, J.-P. Pirard, and Regalbuto, J.R., Synthesis of Very Highly Dispersed Platinum Catalysts Supported on Carbon Xerogels by the Strong Electrostatic Adsorption Method, Journal of Catalysis, 261, 2009, 23.

2008

The Synthesis of Highly Dispersed Noble and Base Metals on Silica via Strong Electrostatic Adsorption: II

Jiao, L., and Regalbuto, J.R., The Synthesis of Highly Dispersed Noble and Base Metals on Silica via Strong Electrostatic Adsorption: II. Mesoporous Silica, Journal of Catalysis, 260, 2008, 342.

The Synthesis of Highly Dispersed Noble and Base Metals on Silica via Strong Electrostatic Adsorption: I

Jiao, L., and Regalbuto, J.R., The Synthesis of Highly Dispersed Noble and Base Metals on Silica via Strong Electrostatic Adsorption: I. Amorphous Silica, Journal of Catalysis 260, 2008, 329.

Preparation of Carbon Supported Cobalt by Electrostatic Adsorption of [Co(NH3)6]Cl3

D’Souza, L., Regalbuto, J.R., and Miller, J.T., Preparation of Carbon Supported Cobalt by Electrostatic Adsorption of [Co(NH3)6]Cl3, Journal of Catalysis 252, 2008, 157.

2007

Preparation of Silica- and Carbon-supported Cobalt by Electrostatic Adsorption of Co(III) Hexaammines

D’Souza, L., Regalbuto, J.R., Miller, J.T., and Kropf, A.J., Preparation of Silica- and Carbon-supported Cobalt by Electrostatic Adsorption of Co(III) Hexaammines, Journal of Catalysis 248, 2007, 165.

2006

Simple, Scientific Syntheses with Common Catalyst Precursors

Regalbuto, J.R., Simple, Scientific Syntheses with Common Catalyst Precursors, Studies in Surface Science and Catalysis 167, 2006, 191.

An Evaluation of Pt Sulfite Acid (PSA) as Precursor for Supported Pt Catalysts

Regalbuto, J.R., Ansel, O., and Miller, J.T., An Evaluation of Pt Sulfite Acid (PSA) as Precursor for Supported Pt Catalysts, Topics in Catalysis 39, 2006, 237.

The Effect of Gold Particle Size on the Au-Au Bond Distance in Supported Catalysts

Miller, J.T., Kropf, A.J., Zha, Y., Regalbuto, J.R., Delannoy, L., Louis, C., Bus, E., and van Bokhoven, J.A., The Effect of Gold Particle Size on the Au-Au Bond Distance in Supported Catalysts, J. Catal. 240, 2006, 222.

2005

Resonant anomalous X-ray reflectivity: A New Structural and Spectroscopic Probe of Metal Adsorption at Mineral-Water Interfaces

Park, Changyong; Fenter, Paul; Sturchio, Regalbuto, John. R., Neil C.; Resonant anomalous X-ray reflectivity: A New Structural and Spectroscopic Probe of Metal Adsorption at Mineral-Water Interfaces, Geochemica et Cosmochimica Acta 69, 2005, A42.

The Nature of “Overexchanged” Copper and Platinum on Zeolites

Schreier, M., Terens, S., Belcher, L. and Regalbuto, J.R., The Nature of “Overexchanged” Copper and Platinum on Zeolites, Nanotechnology 16, 2005, S582.

Understanding Preparation Variables in the Synthesis of Au/Al2O3 using EXAFS and Electron Microscopy

Yang, J.Y., Henao, J. D., Costello, C., Kung, M.C., Kung, H.H., Miller, J.T., Kropf, A.J., Regalbuto, J.R., Kim, J.G., Bore, M., Pham, H.N., Datye, A.K., Laeger, J. D., and Kharas, K., Understanding Preparation Variables in the Synthesis of Au/Al2O3 using EXAFS and Electron Microscopy, Applied Catalysis A: General 291, 2005, 73.

Probing Outer-sphere Adsorption of Aqueous Metal Complexes at the Oxide-Water Interface with Resonant Anomalous X-ray Reflectivity

Park, C., Fenter, P., Sturchio, N., and Regalbuto, J.R., Probing Outer-sphere Adsorption of Aqueous Metal Complexes at the Oxide-Water Interface with Resonant Anomalous X-ray Reflectivity, Physics Review Letters 94, 2005, 076104/1.

2004

The Engineering of Pt Impregnation onto Oxides and Carbon

Hao, X., Quach, L., Korah, J.,and Regalbuto, J. R., The Engineering of Pt Impregnation onto Oxides and Carbon, Journal of Molecular Catalysis 219, 2004, 97.

A Fundamental Study of Pt Ammine Impregnation of Silica 2

Miller, J. T., Kropf, A. J., Schreier, M., and Regalbuto, J.R., A Fundamental Study of Pt Ammine Impregnation of Silica 2. The Effect of Method of Preparation, Loading, and Calcination Temperature on (Reduced) Particle Size, J. Catal. 225, 2004, 203.

A Fundamental Study of Pt Ammine Impregnation of Silica 1

Schreier, M., and Regalbuto, J.R., A Fundamental Study of Pt Ammine Impregnation of Silica 1. The Electrostatic Nature of Pt Adsorption, J. Catal. 225, 2004, 190.

2003

A Further Simplification of the Revised Physical Adsorption (RPA) Model

Hao, X., Spieker, W., and Regalbuto, J. R., A Further Simplification of the Revised Physical Adsorption (RPA) Model, Journal of Colloid and Interface Science 267, 2003, 259.

Korah, J., Spieker, W., and Regalbuto, J. R., Why Ion-Doped, PAC-Altered Silica and Alumina Fail to Influence Platinum Adsorption, Catalysis Letters 85, 2003, 123.

An EXAFS Study of the Coordination Chemistry of Hydrogen Hexachoroplatinate II

Spieker, W., Liu, J., Hao, X., Miller, J. T., Kropf, J., and Regalbuto, J. R., An EXAFS Study of the Coordination Chemistry of Hydrogen Hexachoroplatinate II. Speciation of Complexes Adsorbed onto Alumina, Applied Catalysis A: General 243, 2003, 53.

2002

An EXAFS Study of the Coordination Chemistry of Hydrogen Hexachoroplatinate I

Spieker, W., Liu, J., Miller, J. T., Kropf, J., and Regalbuto, J. R., An EXAFS Study of the Coordination Chemistry of Hydrogen Hexachoroplatinate I. Speciation in Aqueous Solution, Applied Catalysis A: General 232, 2002, 219.

Toward a Molecular Understanding of Noble Metal Catalyst Impregnation

Regalbuto, J. R., Schreier, M., Hao, X., Spieker, W.A., Kim, J.-G., Miller, J. T., and Kropf, J., Toward a Molecular Understanding of Noble Metal Catalyst Impregnation, Studies in Surface Science and Catalysis 143, 2002, 45.

2001

A Fundamental Model of Pt Impregnation onto Alumina

Spieker, W., and Regalbuto, J. R., A Fundamental Model of Pt Impregnation onto Alumina, Chemical Engineering Science 56, 2001, 3491.

2000

Experimental Investigation and Modeling of Platinum Adsorption onto Ion-Modified Silica and Alumina

Spieker, W., Regalbuto, J., Rende, D., Bricker, M., and Chen, Q, Experimental Investigation and Modeling of Platinum Adsorption onto Ion-Modified Silica and Alumina, Studies in Surface Science and Catalysis 130, 2000, 203.

1999

An Experimental Verification of the Physical Nature of CPA Adsorption onto Alumina

Regalbuto, J.R., Shadid, S., Chen, Q., and Bricker, M., An Experimental Verification of the Physical Nature of CPA Adsorption onto Alumina, Journal of Catalysis 184, 1999, 335.

The Bifunctional Reaction Pathway and Dual Kinetic Regimes in NOx SCR by Methane over Cobalt Mordenite Catalysts

Regalbuto, J.R., Zheng, T., and Miller, J. T., The Bifunctional Reaction Pathway and Dual Kinetic Regimes in NOx SCR by Methane over Cobalt Mordenite Catalysts, Catalysis Today 1848, 1999, 1.

1998

A Scientific Description of Pt Adsorption onto Alumina

Regalbuto, J.R., Agashe K., Navada, A., Bricker, M. L., and Chen, Q., A Scientific Description of Pt Adsorption onto Alumina, Studies in Surface Science and Catalysis 118, 1998, 147.

The Role of Acid Sites in Cobalt Zeolite Catalysts for Selective Reduction of Lean NOx

Miller, J., Glusker, E., Peddi, R., Zheng,T., and Regalbuto, J. R., The Role of Acid Sites in Cobalt Zeolite Catalysts for Selective Reduction of Lean NOx, Catalysis Letters 51, 1998, 15.

1997

Selective Adsorption of NOx from Hot Combustion Gases be Ce-Doped CuO/TiO2

Li, W. B., Yang, R. T., Krist, K., and Regalbuto, J. R., Selective Adsorption of NOx from Hot Combustion Gases be Ce-Doped CuO/TiO2, Energy and Fuels 11, 1997, 428.

A Revised Physical Theory for Adsorption of Metal Complexes at Oxide Surfaces

Agashe K., and Regalbuto, J.R., A Revised Physical Theory for Adsorption of Metal Complexes at Oxide Surfaces, Journal of Colloid and Interface Science 185, 1997, 174.

1996

1995

Accurate Determination of Oxide PZC and the Strong Buffering Effect of Oxide Surfaces at Incipient Wetness

Park J.-H., and Regalbuto, J.R., A Simple, Accurate Determination of Oxide PZC and the Strong Buffering Effect of Oxide Surfaces at Incipient Wetness, Journal of Colloid and Interface Science 175, 1995, 239.

Nature of Adsorption Sites on Sulfided Mo Catalysts and Their Selectivity in Chemisorption of Probe Molecules

Hong, Z., and Regalbuto, J. R., Nature of Adsorption Sites on Sulfided Mo Catalysts and Their Selectivity in Chemisorption of Probe Molecules, Journal of Physical Chemistry 99, 1995, 9452.

1994

A Corrected Procedure and Consistent Interpretation for Temperature Programmed Reduction of Supported MoO3

Regalbuto, J.R., and Ha, J.-W., A Corrected Procedure and Consistent Interpretation for Temperature Programmed Reduction of Supported MoO3, Catalysis Letters 29, 1994, 189.

On the Nature of Metal Precursors Adsorbed on Oxide Supports

Santhanam, N., Conforti, T., Spieker, W., and Regalbuto, J.R., On the Nature of Metal Precursors Adsorbed on Oxide Supports, Catalysis Today 21, 1994, 141.

The Retardation of Pt Adsorption Over Oxide Supports at pH Extremes: Oxide Dissolution of High Ionic Strength?

Shah, A., and Regalbuto, J. R., The Retardation of Pt Adsorption Over Oxide Supports at pH Extremes: Oxide Dissolution of High Ionic Strength?, Langmuir 10, 1994, 500.

1993

The Effect of Calcination On Morphology and Hydrogen Spillover in Pt/MoO3, II

Kim, J.-G., and Regalbuto, J.R., The Effect of Calcination On Morphology and Hydrogen Spillover in Pt/MoO3, II. Kinetic Modeling, Journal of Catalysis139, 1993, 175.

The Effect of Calcination On Morphology and Hydrogen Spillover in Pt/MoO3, I

Kim, J.-G., Shyu, J. and Regalbuto, J.R., The Effect of Calcination On Morphology and Hydrogen Spillover in Pt/MoO3, I. Characterization and Kinetics, Journal of Catalysis139, 1993, 153.

1992

The Mixing Characteristics of a MicroBerty Catalytic Reactor

Hannoun, H., and Regalbuto, J.R., The Mixing Characteristics of a MicroBerty Catalytic Reactor, Industrial and Engineering Chemistry Research, 31, 1992, 1288.

The Controlled Dispersion of Silica Supported MoO3: the Role of Ammonia

Datta, A., Ha, J.-W., and Regalbuto, J.R., The Controlled Dispersion of Silica Supported MoO3: the Role of Ammonia, Journal of Catalysis 133, 1992, 55.

1989

TEM and In-Situ EM Study of the Dispersion of Silica Supported MoO3

Datta, A., and Regalbuto, J.R., TEM and In-Situ EM Study of the Dispersion of Silica Supported MoO3, Ultramicroscopy 29, 1989, 233-246.

1988

X-ray Photoemission Studies of Strong Metal-Support Interaction (SMSI): Metal Decoration and Electronic Effects

Fleisch, T.H., Bell, A.T., Regalbuto, J.R., Thomson, R.T., Lane, G.S., Wolf, E.E., and Hicks, R.F., X-ray Photoemission Studies of Strong Metal-Support Interaction (SMSI): Metal Decoration and Electronic Effects, Studies in Surface Science and Catalysis 38, 1988, 791-802.

An Integrated Study of Pt/WO3/SiO2 Catalysts for the NO-CO Reaction III

Regalbuto, J.R., and Wolf, E.E., An Integrated Study of Pt/WO3/SiO2 Catalysts for the NO-CO Reaction III. FTIR Kinetic Study and Correlation of Promotional Effects, Journal of Catalysis 109, 1988, 12-24.

1987

Promotion of Pt/SiO2 Catalysts by WO3 for the NO-CO Reaction

Regalbuto, J.R., and Wolf, E.E., Promotion of Pt/SiO2 Catalysts by WO3 for the NO-CO Reaction. In Crucq, A., and Frennet, A., eds., Catalysis and Automotive Pollution Control, Elsevier, Amsterdam, 1987.

An Integrated Study of Pt/WO3/SiO2 Catalysts for the NO-CO Reaction II. TEM Investigation of Overlayer Formation on Model Pt/WO3/SiO2 Catalysts

Regalbuto, J.R., Allen, C.W., and Wolf, E.E., An Integrated Study of Pt/WO3/SiO2 Catalysts for the NO-CO Reaction II. TEM Investigation of Overlayer Formation on Model Pt/WO3/SiO2 Catalysts, Journal of Catalysis108, 1987, 304-322.

An Integrated Study of Pt/WO3/SiO2 Catalysts for the NO-CO Reaction I. Catalyst Characterization by XRD, Chemisorption, and XPS

Regalbuto, J.R., Fleisch, T.H., and Wolf, E.E., An Integrated Study of Pt/WO3/SiO2 Catalysts for the NO-CO Reaction I. Catalyst Characterization by XRD, Chemisorption, and XPS, Journal of Catalysis 107, 1987, 114-128.

1986

FTIR Studies of Self-sustained Oscillations During the CO-NO-O2 Reaction on Pt/SiO2 Catalysts

Regalbuto, J. R. and Wolf, E. E., FTIR Studies of Self-sustained Oscillations During the CO-NO-O2 Reaction on Pt/SiO2 Catalysts, Chemical Engineering Communications 41, 1986, 315.

1984

Transient FTIR Studies of the CO-NO-O2 Reaction on Pt/SiO2

Regalbuto, J., Kaul, D., and Wolf, E., Transient FTIR Studies of the CO-NO-O2 Reaction on Pt/SiO2. 8th International Congress on Catalysis, Vol. 3, 1984, 253.